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Sieve
- 38-1000 mcm
- ED: sieve pore diameter (varies with particle shape, especially elongated shape)
- Average diameter: weight average diameter
- Function: pass particals through sieves
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Optical Microscope
- 1-1000 mcm
- ED: dp (projected perimeter diamter) or da(projected area diameter)
AD: Number average diamter and weight average diameter (dn, dw)
Function: look at particles through microscope and measure them
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Electron Microscope
0.01-1000 mcm
ED: dp (projected perimeter diamter) or da(projected area diameter)
AD: Number average diamter and weight average diameter (dn, dw)
Function: look at particles through microscope and measure them
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Gravitational Sedimentation method and centrifugal method
- Gravitational sedimentation 10-1000 mcm
- Centrifugal 0.1-1000 mcm
- ED: stokes diamater= dstĀ
- AD: weight average diameter= dw
sedimentation methods:measure how quickly particle sediments, as this is proportional to particle size
note that the centrifugal method is the equation with angular velocity and the natural logarithm (w, and ln)
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Laser light diffraction
- 1-1000 mcm
- analyzes dry or wet samples by shining a light on them and measuring diffraction, the larger the particle the narrower the angle of scattering and the higher the intensity
- ED: area diameter, darea
- AD: volume/weight/number average diameter= dv, dw, da
all of the AD are calculated from the ED
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Dynamic laser light scattering
- 0.01- 2 mcm
- ED: area diamater, darea
- AD: dw, dv, dn (weight volume number)
Function: measures scattering using the principal of Brownian motion of small particles (smaller or comparable to laser light)
Use Stoke-einstein equation , find it as D=kT*10^7/ (3*pi*viscosity*dh)
note that dn is the hydrodynamic diameter
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Coulter Counter
- 0.1-1000 mcm
- usually requires insoluble particles
- ED: volume diameter (regardless of shape-only one that doesn't assume spherical particles)
- AD: volume average diameter, dv
look at tutorial 6 for more detailed explanation
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Cascade inspectors
- <10mcm
- for analyzing aerosols or drug powders
- ED: aerodynamic diameter= da
Can determine MMAD and GSD (mean mass aerodynamic diameter, geometric standard deviation)
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